Fig. 2
Voltammetry of 1-iodohexane (concentration: 9 mM) in 0.1 M TBABF4 using DMF as solvent, recorded at different microelectrodes. Scan rate: 100 mV s−1
(A) Response at a GCE (S = 0.8 mm2)
(B) Response at a palladised platinum electrode (S = 0.8 mm2)
(C) Response at a Cu-Pd modified electrode prepared from a palladium sulfate solution (S = 1.6 mm2)